HRID1593439

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID13389

Pyridin-4-carboxaldehyde

C6H5NO

结构：CON=C1CCc2cc(/C=C/C(=O)c3ccc(OC4CCN(C(=O)OC(C)(C)C)CC4)cc3)ccc21

HCID86595418

未命名化合物

PRODUCTS

生成物

结构：CON=C1CCc2cc(C(CC(=O)c3ccc(OC4CCN(C(=O)OC(C)(C)C)CC4)cc3)C(=O)c3ccncc3)ccc21

HCID86595419

未命名化合物

收率 88%

PROCEDURE

实验过程

The title compound (0.9 g, 88%) was prepared from the product of Step 2 and pyridine-4-carboxaldehyde using the method of Example 1 Step 4; MS(ES+) m/e 597 [M+H]+.

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-b3c2850a2cef4b099efa1e0e0a8b550e
来源数据集: uspto-grants-2007_11
DOI: 10.6084/m9.figshare.5104873.v1
专利: US07297694B2
来源说明: uspto-grants-2007_11

反应 SMILES

[C:1]([O:5][C:6]([N:8]1[CH2:13][CH2:12][CH:11]([O:14][C:15]2[CH:20]=[CH:19][C:18]([C:21](=[O:36])/[CH:22]=[CH:23]/[C:24]3[CH:25]=[C:26]4[C:30](=[CH:31][CH:32]=3)[C:29](=[N:33][O:34][CH3:35])[CH2:28][CH2:27]4)=[CH:17][CH:16]=2)[CH2:10][CH2:9]1)=[O:7])([CH3:4])([CH3:3])[CH3:2].[N:37]1[CH:42]=[CH:41][C:40]([CH:43]=[O:44])=[CH:39][CH:38]=1>>[C:1]([O:5][C:6]([N:8]1[CH2:9][CH2:10][CH:11]([O:14][C:15]2[CH:20]=[CH:19][C:18]([C:21](=[O:36])[CH2:22][CH:23]([C:24]3[CH:25]=[C:26]4[C:30](=[CH:31][CH:32]=3)[C:29](=[N:33][O:34][CH3:35])[CH2:28][CH2:27]4)[C:43](=[O:44])[C:40]3[CH:41]=[CH:42][N:37]=[CH:38][CH:39]=3)=[CH:17][CH:16]=2)[CH2:12][CH2:13]1)=[O:7])([CH3:4])([CH3:3])[CH3:2]