HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Methyl 2-(4-hydroxyphenoxy)-2-methylbutanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 86604654 | HCID 86604654 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Methyl 2-(4-hydroxyphenoxy)-2-methylbutanoate | HCID 21111741 | — |
Reaction Steps
A solution of methyl-(4-(benzyloxy)phenoxy)-2-methylbutanoate (32 g) in 100 mL MeOH was hydrogenated using 10% Pd/C at 40 psi. The mixture was filtered through a pad of celite to remove the catalyst. The filtrate was concentrated to afford thick oily residue (21 g, quantitative).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07297715B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-86b717274ce14d5da68fccbb693d3510 |
| Source note | uspto-grants-2007_11 |