HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67206080, compound → HCID 66812220, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67206080 | HCID 67206080 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 66812220 | HCID 66812220 | 110.3% |
Reaction Steps
To a solution of benzyl [(3R)-6-fluoro-2,3,4,9-tetrahydro-1H-carbazol-3-yl]carbamate (240 mg, 0.71 mmol) in ethanol was added 20 mg of 10% palladium on carbon. Hydrogenation at 50 psi overnight, followed by filtration and concentration of the filtrate, afforded 160 mg of the title compound as an off-white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07297704B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-f96f671da73b446bb9853e9aa30ce5e9 |
| Source note | uspto-grants-2007_11 |