HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropylethylamine → HCID 68682074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropylethylamine | HCID 81531 | — |
| Reactant | 5-(4-Bromomethylphenyl)-2-methyl-2H-tetrazole | HCID 589329 | — |
| Reactant | HCID 131726693 | HCID 131726693 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Product | HCID 68682074 | HCID 68682074 | — |
Reaction Steps
This compound was prepared in a manner analogous to that of Step E of Example 3, using 7.0 grams (0.026 mole) of 4-piperidyl[4-(trifluoromethoxy)phenyl]methanol, hydrochloride, 6.8 grams (0.026 mole) of 5-[4-(bromomethyl)phenyl]-2-methyl-1,2,3,4-tetraazole (prepared in a manner analogous to that of Steps A–C of Example 4), and 9.9 grams (0.077 mole) of N,N-diisopropylethylamine in about 40 mL of DMSO. The NMR spectrum was consistent with the proposed structure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07300946B2 |
| Source dataset | uspto-grants-2007_11 |
| ORD ID | ord-e4c5c0643bc84807b5ec2b2a41b3ba13 |
| Source note | uspto-grants-2007_11 |