4-Toluenesulfonyl chloride → HCID 9883379, compound

HRID 1594707Notes

Reaction equation

HRID 1594707 reaction equation
[C:1]1([CH3:12])[CH:6]=[CH:5][C:4]([CH:7]2[CH2:11][CH2:10][CH2:9][NH:8]2)=[CH:3][CH:2]=1.[C:13]1([CH3:23])[CH:18]=[CH:17][C:16]([S:19](Cl)(=[O:21])=[O:20])=[CH:15][CH:14]=1>>[C:13]1([CH3:23])[CH:18]=[CH:17][C:16]([S:19]([N:8]2[CH2:9][CH2:10][CH2:11][CH:7]2[C:4]2[CH:5]=[CH:6][C:1]([CH3:12])=[CH:2][CH:3]=2)(=[O:21])=[O:20])=[CH:15][CH:14]=1

Participants

3

Reactant 2

HCID 73974-Toluenesulfonyl chlorideHCID 35631342-(4-methylphenyl)pyrrolidine

Product 1

HCID 9883379HCID 9883379, compound

Procedure

The title compound, white solid, m.p. 124° C. and MS: m/e=315 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-p-tolyl-pyrrolidine and toluene-4-sulfonyl chloride.

Sources & evidence

ORD record
ord-af47a4f06a8a44fdb0fe2427d2b2c9e5
Source dataset
uspto-grants-2001_09
Patent number
US06284785B1

Reaction notes

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