4-Toluenesulfonyl chloride → HCID 21706728, compound

HRID 1594752Notes

Reaction equation

HRID 1594752 reaction equation
[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[CH2:10][CH2:9][CH2:8][NH:7]1.[C:11]1([CH3:21])[CH:16]=[CH:15][C:14]([S:17](Cl)(=[O:19])=[O:18])=[CH:13][CH:12]=1>>[O:1]1[CH:5]=[CH:4][CH:3]=[C:2]1[CH:6]1[CH2:10][CH2:9][CH2:8][N:7]1[S:17]([C:14]1[CH:15]=[CH:16][C:11]([CH3:21])=[CH:12][CH:13]=1)(=[O:19])=[O:18]

Participants

3

Reactant 2

HCID 73974-Toluenesulfonyl chlorideHCID 36759882-(furan-2-yl)pyrrolidine

Product 1

HCID 21706728HCID 21706728, compound

Procedure

The title compound, white solid, m.p. 58° C. and MS: m/e=291 (M+) was prepared in accordance with the general method of example 1e from (RS)-2-furan-2-yl-pyrrolidine and toluene-4-sulfonyl chloride.

Sources & evidence

ORD record
ord-cb481302f3d540e1addeffccfd88c9da
Source dataset
uspto-grants-2001_09
Patent number
US06284785B1

Reaction notes

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