Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | 2-Bromopropane | HCID 6358 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,4,6-tris(2,4-dihydroxyphenyl)-1,3,5-triazine | HCID 135714880 | — |
| Solvent | Diglyme | HCID 8150 | — |
| Product | HCID 136393229 | HCID 136393229 | — |
Reaction Steps
A mixture of 50.0 g (0.123 mol ) of 2,4,6-tris(2′,4′-dihydroxyphenyl)-1,3,5-triazine, 54.6 g (0.395 mol) of potassium carbonate, 1.0 g (0.006 mol) of potassium iodide (Merck, 99.0%) and 50.1 g (0.407 mol) of isopropyl bromide (Fluka, 99.0%) in 200 ml of diethylene glycol dimethyl ether (Diglyme, Merck, >99%) is held with stirring at 140° C. under a pressure of 3.8 bar for 24 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06284821B1 |
|---|
| Source dataset | uspto-grants-2001_09 |
|---|
| ORD ID | ord-0ca58f4b9d164807aff4b8a318f86ec3 |
|---|
| Source note | uspto-grants-2001_09 |
|---|
