HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → 5-Diethylamino-2-nitrosophenol hydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | 3-(Diethylamino)phenol | HCID 7062 | — |
| Reactant | Isoamyl Nitrite | HCID 8053 | — |
| Solvent | 1-Propanol | HCID 1031 | — |
| Product | 5-Diethylamino-2-nitrosophenol hydrochloride | HCID 33253 | — |
Reaction Steps
0.1 mol of 3-diethylaminophenol are dissolved in 50 ml of n-propanol saturated with gaseous hydrogen chloride and, at 0° C., admixed dropwise and with stirring with 0.1 mol of isoamyl nitrite. Stirring is continued for another hour and the reaction solution is then admixed with diethyl ether, and the product which is formed is isolated by filtration with suction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06284889B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-eaae6b0564aa4c219eb57f5092b97c57 |
| Source note | uspto-grants-2001_09 |