Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Fluoride | HCID 5235 | — |
| Reactant | Phenyl chloroformate | HCID 15891 | — |
| Reactant | 15-Crown-5 | HCID 36336 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Phenyl Fluoroformate | HCID 11815898 | — |
Reaction Steps
To a solution of phenylchloroformate in acetonitrile is charged sodium fluoride. To this mixture is charged the 15-crown-5 (“15C5”) at ambient temperature. The reaction mixture is then heated to 40° C. for approximately 16 hrs. Reaction completion is monitored by gas chromatography (“G.C.”).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06284911B1 |
|---|
| Source dataset | uspto-grants-2001_09 |
|---|
| ORD ID | ord-8b9ce016ec564ff58f9729c1d8df04f0 |
|---|
| Source note | uspto-grants-2001_09 |
|---|
