HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-chloropropane → HCID 12146432, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-chloropropane | HCID 8006 | — |
| Reactant | HCID 12044319 | HCID 12044319 | — |
| Reactant | Potassium tert-butoxide | HCID 23665647 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 12146432 | HCID 12146432 | 50.3% |
Reaction Steps
Using Compound 12 (0.96 g, 5 mmole), potassium t-butoxide (1.12 g, 10 mmole), 1-bromo-3-chloropropane (3.46 g, 22 mmole) and THF (50 ml), the title compound (676 mg) was obtained in a similar manner as in Preparation Example 6 (yield: 50%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288056B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-3feb865341974c49925e957394e13ff3 |
| Source note | uspto-grants-2001_09 |