HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyanamide → HCID 178453081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyanamide | HCID 9864 | — |
| Reactant | HCID 70235112 | HCID 70235112 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178453081 | HCID 178453081 | — |
Reaction Steps
10 mmol of di-(tert-butyl) 4-aminobenzylimidodicarbonate and 100 mmol of cyanamide are heated at reflux for 2 days in 80 ml of anhydrous ethanol. Removal of the ethanol by evaporation, and purification by chromatography on silica, yield the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288077B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-5b049efca06b40b7bb801bb8774b6c85 |
| Source note | uspto-grants-2001_09 |