HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 178450793, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 178451309 | HCID 178451309 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178450793 | HCID 178450793 | 41.8% |
Reaction Steps
tert-Butyl 2-hydroxyimino-3-oxo-3-(3-pyridyl)propionate (4.1 g), benzylamine (3.5 g) and acetonitrile (80 ml) were reacted and treated in the same manner as in Starting Material Synthetic Example 5 to give tert-butyl 2-phenyl-5-(3-pyridyl)imidazole-4-carboxylate (2.2 g), melting point 196-197° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288061B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-3608a990c9574e10b344e6e0b52131be |
| Source note | uspto-grants-2001_09 |