HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 178450792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | HCID 178451308 | HCID 178451308 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 178450792 | HCID 178450792 | 23.4% |
Reaction Steps
tert-Butyl 2-hydroxyimino-3-oxo-3-(2-pyridyl)propionate (6.0 g) and benzylamine (5.7 g) were dissolved in acetonitrile (100 ml), and the mixture was reacted and treated in the same manner as in Starting Material Synthetic Example 5 to give tert-butyl 2-phenyl-5-(2-pyridyl)imidazole-4-carboxylate (1.8 g), melting point 211-213° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288061B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-b38163353d234f67a7d33d03d172361f |
| Source note | uspto-grants-2001_09 |