HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Methoxybenzylamine → HCID 178489897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Methoxybenzylamine | HCID 21156 | — |
| Reactant | HCID 178451310 | HCID 178451310 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 178489897 | HCID 178489897 | 31.2% |
Reaction Steps
tert-Butyl 2-hydroxyimino-3-oxo-3-(4-pyridyl)propionate (3.2 g) and 3-methoxybenzylamine (2.1 g) were dissolved in toluene (120 ml), and the mixture was reacted and treated in the same manner as in Starting Material Synthetic Example 10 to give tert-butyl 2-(3-methoxyphenyl)-5-(4-pyridyl)imidazole-4-carboxylate (1.4 g), melting point 197-199° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288061B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-1dcc40747ff943dfbecd29c967fb4815 |
| Source note | uspto-grants-2001_09 |