HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Pyridinemethanamine → HCID 178470220, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Pyridinemethanamine | HCID 77317 | — |
| Edukt | HCID 178472891 | HCID 178472891 | — |
| Lösungsmittel | O-Xylene | HCID 7237 | — |
| Produkt | HCID 178470220 | HCID 178470220 | 395,1% |
Reaktionsschritte
Ethyl 2-hydroxyimino-3-(4-methylphenyl)-3-oxopropionate (10.5 g) and 4-aminomethylpyridine (5.8 g) were dissolved in xylene (100 ml), and the mixture was reacted and treated in the same manner as in Starting Material Synthetic Example 1 to give ethyl 5-(4-methylphenyl)-2-(4-pyridyl)imidazole-4-carboxylate (54.2 g), melting point 182-185° C.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06288061B1 |
| Quelldatensatz | uspto-grants-2001_09 |
| ORD ID | ord-0edcf67e3f364e86ac4595f59cc055d0 |
| Quellennotiz | uspto-grants-2001_09 |