HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178489908, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178470206 | HCID 178470206 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178489908 | HCID 178489908 | 101.1% |
Reaction Steps
Ethyl 5-(3-methoxyphenyl)-2-(4-nitrophenyl)imidazole-4-carboxylate (45.1 g) was dissolved in ethanol. 1 M Sodium hydroxide solution was added and the mixture was reacted and treated in the same manner as in Starting Material Synthetic Example 2 to give 5-(3-methoxyphenyl)-2-(4-nitrophenyl)imidazole-4-carboxylic acid (42.1 g), melting point 116-118° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288061B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-77b486001fcf456aa72eaadaeeb135fe |
| Source note | uspto-grants-2001_09 |