HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzylamine → HCID 178475836, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzylamine | HCID 29147 | — |
| Reactant | HCID 178475845 | HCID 178475845 | — |
| Product | HCID 178475836 | HCID 178475836 | 15.3% |
Reaction Steps
tert-Butyl 3-(4-acetoxymethylphenyl)-2-hydroxyimino-3-oxopropionate (33.9 g) and 4-nitrobenzylamine (19.3 g) were reacted and treated in the same manner as in Starting Material Synthetic Example 1 to give tert-butyl 5-(4-acetoxymethylphenyl)-2-(4-nitrophenyl)-imidazole-4-carboxylate (7.07 g), melting point 178-180° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288061B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-df777a481833423a9b5741e764222159 |
| Source note | uspto-grants-2001_09 |