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HRID1595360

反应详情

EQUATION

反应方程式

HRID 1595360 的结构方程式

REACTANTS

反应物

2
结构：NCc1cccc([N+](=O)[O-])c1
HCID122722

1-(3-Nitrophenyl)methanamine

C7H8N2O2

结构：CCOC(=O)C(=NO)C(=O)c1ccc(OC)cc1
HCID178472900

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1nc(-c2cccc([N+](=O)[O-])c2)[nH]c1-c1ccc(OC)cc1
HCID178470188

未命名化合物

收率 45.5%

PROCEDURE

实验过程

Ethyl 2-hydroxyimino-3-(4-methoxyphenyl)-3-oxopropionate (20.0 g) and 3-nitrobenzylamine (15.0 g) were reacted and treated in the same manner as in Starting Material Synthetic Example 10 to give ethyl 5-(4-methoxyphenyl)-2-(3-nitrophenyl)imidazole-4-carboxylate (13.3 g), melting point 208-210° C.

WORKUP

后处理

  1. additiontreated in the same manner as