HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-([4-Benzyloxyphenyl]methyl)oxazolidine-2,4-dione → 5-([4-Hydroxyphenyl]methyl)oxazolidine-2,4-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-([4-Benzyloxyphenyl]methyl)oxazolidine-2,4-dione | HCID 10447330 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 5-([4-Hydroxyphenyl]methyl)oxazolidine-2,4-dione | HCID 10352968 | 94% |
Reaction Steps
2.75 g (9.25 mmole) 5-([4-benzyloxyphenyl]methyl)oxazolidine-2,4-dione was hydrogenated at 50 psi over night in 1,4-dioxan using Pd/C as catalyst to give 1.8 g (yield 94%) of 5-([4-hydroxyphenyl]methyl)oxazolidine-2,4-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288096B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-e4330ed7ded746cc88baa728f37b0f4c |
| Source note | uspto-grants-2001_09 |