HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2,4-Bis(benzyloxy)phenyl)ethanol → 4-(2-Hydroxyethyl)benzene-1,3-diol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2,4-Bis(benzyloxy)phenyl)ethanol | HCID 14802909 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | 4-(2-Hydroxyethyl)benzene-1,3-diol | HCID 13486360 | 99.3% |
Reaction Steps
3.7 g (11.1 mmole) 2-[2,4-di(benzyloxy)phenyl]-1-ethanol was hydrogenated in 100 ml ethyl acetate using Pd/C (10%) as catalyst. The reaction mixture was filtered and the filtrate was evaporated in vacuo to give 1.7 g (yield 99%) of 2-(2,4-dihydroxyphenyl)-1-ethanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06288096B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-f6ad53db194f46bead28d4ad27118587 |
| Source note | uspto-grants-2001_09 |