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HRID1595517

反应详情

EQUATION

反应方程式

HRID 1595517 的结构方程式

REACTANTS

反应物

1
反应SMILES：CC(C)(C)NC(=O)Oc1ccc(CCOc2ccc(C=C3SC(=O)NC3=O)cc2)cc1
HCID54298639

未命名化合物

PRODUCTS

产物

1
反应SMILES：CC(C)(C)NC(=O)Oc1ccc(CCOc2ccc(CC3SC(=O)NC3=O)cc2)cc1
HCID21705017

未命名化合物

收率 99.5%

AUXILIARIES

试剂、催化剂与溶剂

1
反应SMILES：CCOC(C)=O
溶剂HCID8857

Ethyl acetate

C4H8O2

PROCEDURE

实验过程

1 g (2.27 mmole) 5-(4-[2-(4-tert-butylaminocarbonyloxyphenyl)ethoxy]benzylidene)thiazolidine-2,4-dione was hydrogenated on Pd/C (5%) in ethyl acetate at atmospheric pressure over night. The catalyst was filtered off and the solvent was evaporated in vacuo to give 1 g (yield 99%) of the desired product.

WORKUP

后处理

  1. filtrationThe catalyst was filtered off
  2. customthe solvent was evaporated in vacuo