HRID1596017

反应详情

EQUATION

反应方程式

HRID 1596017 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A two-phase mixture of 3-(benzhydrylideneamino)-8-oxabicyclo[3.2.1]octane-3-carboxylic acid benzyl ester (3.9 mmole) in aqueous 1N hydrochloric acid solution (100 mL.) and diethyl ether (100 mL) is stirred at room temperature overnight. The aqueous layer ifs concentrated to provide the title compound.

WORKUP

后处理

  1. concentrationThe aqueous layer ifs concentrated