HRID1596182

反应详情

EQUATION

反应方程式

HRID 1596182 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of (1-benzhydrylazetidin-3-ylidene)-acetic acid ethyl ester (5.0 g, 16 mmol) in ethanol (200 mL) was added palladium hydroxide on carbon (1.5 g). This mixture was vigorously shaken under a 50 psi hydrogen atmosphere for 24 hrs, then filtered and concentrated to give an oil, used without additional purification.

WORKUP

后处理

  1. filtrationfiltered
  2. concentrationconcentrated
  3. customto give an oil
  4. customused without additional purification