Thiobenzamide → HCID 21702073, compound

HRID 1596423Notes

Reaction equation

HRID 1596423 reaction equation
[Br:1][CH:2]1[CH2:10][C:9]2[C:4](=[CH:5][CH:6]=[C:7]([O:11][CH2:12][C:13]([F:16])([F:15])[F:14])[CH:8]=2)[C:3]1=[O:17].[C:18]([NH2:26])(=[S:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[BrH:1].[C:19]1([C:18]2[S:25][CH:2]3[CH2:10][C:9]4[CH:8]=[C:7]([O:11][CH2:12][C:13]([F:16])([F:15])[F:14])[CH:6]=[CH:5][C:4]=4[C:3]3([OH:17])[N:26]=2)[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

3

Reactant 2

HCID 683563ThiobenzamideHCID 18347148HCID 18347148, compound

Product 1

HCID 21702073HCID 21702073, compound

Procedure

This compound is prepared analogously to the process described in Example 1c using 2-bromo-5-(2,2,2-trifluoroethoxy)indan-1-one and thiobenzamide; melting point: 240-246° C.

Workup

  1. customThis compound is prepared analogously to the process

Sources & evidence

ORD record
ord-d48a93340eb84f3aa117e19ef515c04d
Source dataset
uspto-grants-2001_09
Patent number
US06291486B1

Reaction notes

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