反应详情

mCPBA (15.9 g; 65 mmol) was added to a stirred solution of 4-(4′-cyanophenoxy)but-1-ene (7.5 g; 56 mmol; prepared according to the method described in J. Chem. Soc. Perkin Trans. 1, 9 (1992) 1145-1148) in CH2Cl2 (175 mL) and the reaction mixture was stirred at room temperature for 4 h. The reaction mixture was washed with NaHCO3 (aq.) and the organic layer separated, dried and concentrated to give the sub-title compound (7.23 g; 38 mmol).

1. customprepared
2. washThe reaction mixture was washed with NaHCO3 (aq.)
3. customthe organic layer separated
4. customdried
5. concentrationconcentrated