HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanethiol → HCID 21702000, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanethiol | HCID 6343 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | HCID 21702023 | HCID 21702023 | — |
| Product | HCID 21702000 | HCID 21702000 | 63.8% |
Reaction Steps
[6-Methoxy-2-(4-methoxyphenyl)benzo[b]thiophen-3-yl][4-(2-methoxy-3-hexylaminopropoxy)phenyl]methanone (340 mg, 0.62 mmol) was converted to 200 mg of the title compound by the procedure of Example 32 using 0.23 mL (3.1 mmol) of ethanethiol 660 mg (5.0 mmol) of aluminum chloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06291484B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-b3f54468eebc477782374d5a06833abf |
| Source note | uspto-grants-2001_09 |