Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hexane | HCID 8058 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 21702494 | HCID 21702494 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21702555 | HCID 21702555 | 42,568.398% |
Reaction Steps
1-(3-Fluorophenyl)-1,4-pentandione (23 g, 0.12 mmol) was dissolved in water (550 ml) containing 11 g of sodium hydroxide and the solution was stirred at 100° C. for 3 hours. After cooling to 0° C. the resultant brown crystals were collected by filtration and washed with water. The title compound (9 g, 45% yield) was obtained by recrystallization from hexane as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06291520B1 |
|---|
| Source dataset | uspto-grants-2001_09 |
|---|
| ORD ID | ord-48cff1d21022410d9fe8ec42a01f1a89 |
|---|
| Source note | uspto-grants-2001_09 |
|---|
