HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53772014, compound → HCID 53876066, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53772014 | HCID 53772014 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53876066 | HCID 53876066 | — |
Reaction Steps
To a solution of t-butyl (5-acetyl-2-benzyloxyphenoxy)-acetate (2.0 g, 5.6 mmol) in EtOH (25 mL) is added 10% Pd/C (0.10 g), and the mixture is hydrogenated at 1 atm for 1.25 hours. Filtration through celite, followed by solvent removal in vacuo yields t-butyl (5-acetyl-2-hydroxyphenoxy)-acetate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06291530B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-1c4a729683c04f80949545b27ff8b3f5 |
| Source note | uspto-grants-2001_09 |