HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Naphthoyl chloride → HCID 15538692, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Naphthoyl chloride | HCID 75246 | — |
| Reactant | HCID 23502535 | HCID 23502535 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 15538692 | HCID 15538692 | — |
Reaction Steps
3-[5-Amino-7-fluoro-2H-1,4-benzoxazine-3(4H)-on-6-yl]-1-methyl-6-trifluoromethyl-2,4-(1H, 3H)-pyrimidinedione (0.37 g) and 2-naphthoyl chloride (0.21 g) were mixed in dioxane (15 ml) and the mixture was refluxed for 6 hr. After evaporation of solvent, the residue was recrystallized from toluene (0.20 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294503B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-0d8f7886bc0546399b7ea3a0ee47fe1a |
| Source note | uspto-grants-2001_09 |