HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 21700096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 21700064 | HCID 21700064 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 21700096 | HCID 21700096 | 96.1% |
Reaction Steps
A suspension of Example 126A (850 mg, 2.28 mmol) in ethanol (100 mL) at ambient temperature was treated with sodium borohydride (103 mg, 2.74 mmol), stirred for 30 minutes, treated with water, extracted with ethyl acetate, dried (Na2SO4) and concentrated to provide 820 mg (96%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294573B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-5e5492c2aea7433eac3f0afae72a3400 |
| Source note | uspto-grants-2001_09 |