HuagongsheHuagongshe Chemistry Print Report · For research reference only
196809-80-0 → HCID 54388575, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 196809-80-0 | HCID 1810294 | — |
| Reactant | Methyl 4-bromo-3-oxopentanoate | HCID 9815681 | — |
| Product | HCID 54388575 | HCID 54388575 | 50.8% |
Reaction Steps
The title compound (854 mg) was prepared from 1.0 g (6.20 mmol) of 3-dimethylaminopropyl thiourea and 1.30 g (6.20 mmol) of methyl 4-bromo-3-oxo-pentanoate according to the method of Intermediate 45: low resolution MS (FAB)m/e 272 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06294580B1 |
| Source dataset | uspto-grants-2001_09 |
| ORD ID | ord-3a08ee800cde48339ceb25e9fc99ad74 |
| Source note | uspto-grants-2001_09 |