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HRID1597463

反应详情

EQUATION

反应方程式

HRID 1597463 的结构方程式

REACTANTS

反应物

2
结构：COc1ccc(C(=O)C2CCCCC2=O)cc1
HCID244418

2-(4-methoxybenzoyl)cyclohexanone

C14H16O3

结构：COC(=O)[C@@H](N)Cc1ccc(OCc2ccccc2)cc1.Cl
HCID12616037

未命名化合物

PRODUCTS

生成物

1
结构：COC(=O)C(Cc1ccc(O)cc1)Nc1ccccc1C(=O)c1ccc(OC)cc1
HCID54539013

未命名化合物

收率 28.5%

PROCEDURE

实验过程

The title compound (2.31 g) was prepared from 4.64 g (20 mmol) of 2-(4-methoxybenzoyl)-cyclohexanone (Howard, A. S. et. al. Tetrahedron Lett. 1979, (15), 1339-40) and 6.43 g (20 mmol) of O-benzyl-L-tyrosine methyl ester hydrochloride as a yellow solid as described for Intermediate 161: low resolution MS (Cl) m/e 406 (MH+).