Dimethyl Sulfate → HCID 86752357, compound

HRID 1597713Notes

Reaction equation

HRID 1597713 reaction equation
[S:1]([O:6]C)([O:4][CH3:5])(=[O:3])=[O:2].O.[N+:9]([C:12]1[CH:17]=[C:16]([NH2:18])[C:15]([S:19][CH2:20][CH2:21][N:22]([CH3:24])[CH3:23])=[CH:14][C:13]=1[NH2:25])([O-:11])=[O:10]>C(OCC)(=O)C>[CH3:5][O:4][S:1]([O-:6])(=[O:3])=[O:2].[N+:9]([C:12]1[CH:17]=[C:16]([NH2:18])[C:15]([S:19][CH2:20][CH2:21][N+:22]([CH3:5])([CH3:23])[CH3:24])=[CH:14][C:13]=1[NH2:25])([O-:11])=[O:10]

Participants

4

Reactant 2

HCID 6497Dimethyl SulfateHCID 86752358HCID 86752358, compound

Product 1

HCID 86752357HCID 86752357, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

4.8 ml (0.05 mol) of dimethyl sulphate were added to a suspension, at room temperature, of 13.7 g (0.05 mol) of 2-nitro-5-(dimethylaminoethylthio)paraphenylenediamine monohydrate, prepared in Example 16, in 250 ml of ethyl acetate.

Sources & evidence

ORD record
ord-ffbef0e1f5064bf59f5c641bbea15c0c
Source dataset
uspto-grants-1998_04
Patent number
US05735910

Reaction notes

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