HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-6,7-dimethoxyquinazoline → HCID 18932776, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-6,7-dimethoxyquinazoline | HCID 2769364 | — |
| Reactant | HCID 12369276 | HCID 12369276 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 18932776 | HCID 18932776 | 93% |
Reaction Steps
Utilizing a procedure analogous to that described in Example 1, this product was prepared in 93% yield from 6,7-dihydro-5H-[1,3]dioxolo[4,5-f]indole (1.1 eq.), and 4-chloro-6,7-dimethoxy-quinazoline (1.0 eq) in i-PrOH. (M.P. 225°-228° C. (dec); LC-MS: 352 (MH+); anal. RP18-HPLC RT: 3.91 min.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736534 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-8f30caa16e0e4e83aab49145607115bb |
| Source note | uspto-grants-1998_04 |