HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chloro-6,7-dimethoxyquinazoline → HCID 18932755, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chloro-6,7-dimethoxyquinazoline | HCID 2769364 | — |
| Reactant | HCID 18932780 | HCID 18932780 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 18932755 | HCID 18932755 | 96% |
Reaction Steps
Utilizing a procedure analogous to that described in Example 1, this product was prepared in 96% yield from [2,3-dihydro-1H-indol-5-yl]-(1-methyl-heptyl)-amine (1.1 eq.), and 4-chloro-6,7-dimethoxy-quinazoline (1.0 eq) in i-PrOH. (M.P. 61°-63° C.; GC-MS: 434 (M+); anal. RP18-HPLC RT: 6.91 min.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736534 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-2e570cc2b1bd4566a3c7a0d4410f1c58 |
| Source note | uspto-grants-1998_04 |