HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67672704, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 6999482 | HCID 6999482 | — |
| Product | HCID 67672704 | HCID 67672704 | — |
Reaction Steps
±-trans-Cyclohexane-1,3-diamine: 22.9 g of the BOC derivative are introduced into 1 00 ml of trifluoroacetic acid while cooling with ice. The mixture is left at RT for 4 hours, evaporated and the residue is recrystallized from 200 ml of acetonitrite. 8.5 g of ±-trans-cyclohexane-1,3-diamine trifluoroacetate, m.p. 200° C. (sintering) are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736557 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-ffc6130b383646acb455c97c1240bde5 |
| Source note | uspto-grants-1998_04 |