HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl Isocyanate → 5-Cyano-3-methyl-6-methylthio-1-phenyl-2,4(1H,3H)-pyrimidinedione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl Isocyanate | HCID 12228 | — |
| Reactant | Ethyl 3-anilino-2-cyano-3-methylsulfanylprop-2-enoate | HCID 4200299 | — |
| Product | 5-Cyano-3-methyl-6-methylthio-1-phenyl-2,4(1H,3H)-pyrimidinedione | HCID 18933452 | 27% |
Reaction Steps
This compound was synthesized from ethyl 2-cyano-3-methylthio-3-phenylaminoacrylate and methyl isocyanate according to the same process as described in Example 92b. Yield=27%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736550 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-e2c1daaeb9d6451384ae9c2525971d3e |
| Source note | uspto-grants-1998_04 |