HCID 67629372, compound → HCID 54397865, compound

Participants

Reaction Steps

4-Benzyl-2(S)-n-butyl-1-(2,3-dimethylbenzoyl)piperazine (0.93 g, 2.55 mmol) was dissolved in methanol and hydrogenated in a Parr apparatus under 60 psi hydrogen in the presence of 10% Pd/C (0.186 g) for 24 h. The catalyst was removed by filtration through Celite, and the solvent removed in vacuo to obtain the title compound (0.818 g).

Provenance & Evidence