HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Naphthoic acid → HCID 22884139, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Naphthoic acid | HCID 6847 | — |
| Reactant | 1-Hydroxybenzotriazole | HCID 75771 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | HCID 22884140 | HCID 22884140 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22884139 | HCID 22884139 | — |
Reaction Steps
The title compound was prepared according to the procedure described for Example 1, Step A except using 1-tert-butoxycarbonyl-2(S)-(3-methoxypropyl)piperazine (0.215 g, 0.832 mmol), naphthalene-1-carboxylic acid (0.143 g, 0.83 mmol), HOBT (0.128 g, 0.83 mmol), EDC.HCl (0.160 g, 0.83 mmol) in DMF (5 mL). The title compound was obtained as an oil (0.310 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736539 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-3fc888475a96402d96a86d345e26d584 |
| Source note | uspto-grants-1998_04 |