Potassium bisulfate → HCID 22884155, compound

Participants

Reaction Steps

The title compound was prepareded according to the procedure described in Example 1, Step C, except using N-methoxy-N-methyl 2(R)-tert-butoxycarbonylaminohexanamide (4.08 g, 14.89 mmol), lithium aluminum hydride (0.621 g, 16.37 mmol), in ether (200 mL), followed by potassium hydrogen sulfate (4.05 g, 29.78 mmol) workup. The title compound was obtained as a clear oil, 3.28 g. NMR (CDCl3, 300 MHz) δ 9.6 (1H, s), 5.04 (1H, bs), 4.23 (1H, m), 1.15-2.0 (15H, m), 0.9 (3H, m).

Provenance & Evidence