HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Hydroxybenzotriazole → HCID 22884173, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Hydroxybenzotriazole | HCID 75771 | — |
| Reactant | (Benzylamino)acetaldehyde diethyl acetal | HCID 521961 | — |
| Reactant | 1,3-Propanediamine, N'-(ethylcarbonimidoyl)-N,N-dimethyl-, monohydrochloride | HCID 2723939 | — |
| Reactant | N-tert-Butoxycarbonyl-L-norleucine | HCID 2733747 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 22884173 | HCID 22884173 | — |
Reaction Steps
The title compound was prepared according to the procedure described in Example 1, Step A except using 2(S)-t-butoxycarbonylaminohexanoic acid (1.98 g, 8.57 mmol), EDC.HCl (1.96 g, 10.28 mmol), N-benzyl 2-aminoacetaldehyde diethyl acetal (1.91 g, 8.57 mmol), HOBT (1.15 g, 8.57 mmol) in DMF. The title compound was obtained as a yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05736539 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-5b32dfcae3b54c93b092536bbb58e13b |
| Source note | uspto-grants-1998_04 |