Hydrochloric Acid → HCID 131720594, compound

HRID 1598632Notes

Reaction equation

HRID 1598632 reaction equation
[NH2:1][C:2]([NH2:24])=[N:3][C:4](=[O:23])[C:5]1[CH:10]=[C:9]([S:11]([CH3:14])(=[O:13])=[O:12])[C:8]([N:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]2)=[CH:7][C:6]=1[CH2:21][CH3:22].[ClH:25]>O>[ClH:25].[NH2:24][C:2]([NH2:1])=[N:3][C:4](=[O:23])[C:5]1[CH:10]=[C:9]([S:11]([CH3:14])(=[O:13])=[O:12])[C:8]([N:15]2[CH2:20][CH2:19][CH2:18][CH2:17][CH2:16]2)=[CH:7][C:6]=1[CH2:21][CH3:22]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 9841436HCID 9841436, compound

Product 1

HCID 131720594HCID 131720594, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

4 g of N-diaminomethylene-2-ethyl-4-piperidino-5-methylsulfonylbenzamide [obtainable according to Example 1] are suspended in 100 ml of water, dissolved with the stoichiometric quantity of 1-molar aqueous HCl solution and then freeze-dried to give N-diaminomethylene-2-ethyl-4-piperidino-5-methylsulfonylbenzamide, hydrochloride, m.p.>250°.

Workup

  1. customfreeze-dried

Sources & evidence

ORD record
ord-a2bf448ebe6e4f338712f0940169006a
Source dataset
uspto-grants-1998_04
Patent number
US05739142

Reaction notes

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