HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrogen Bromide → HCID 376124, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrogen Bromide | HCID 260 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 18930606 | HCID 18930606 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 376124 | HCID 376124 | — |
Reaction Steps
A mixture of N-benzyloxycarbonyl derivative (2a, 3.13 g, 8.06 mmol) obtained in Preparation 1 and a solution of 30% hydrobromic acid in acetic acid is stirred for 1 hour. Excess ether is added, and the resultant precipitate is filtered off. After washing with ether, it is dried to obtain 2.50 g (92%) of hydrobromate (compound 3a).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05739162 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-6d57f4745829462e90f9b08758c91d70 |
| Source note | uspto-grants-1998_04 |