HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylamine → 1,2-Dihexadecyloxy-3-dimethylamino glycerol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylamine | HCID 674 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 54034972 | HCID 54034972 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | 1,2-Dihexadecyloxy-3-dimethylamino glycerol | HCID 19083693 | — |
Reaction Steps
900 mg of 3-bromo-1,2-dihexadecyloxy glycerol was dissolved in 30 ml chloroform in a 100 ml round bottom flask. 720 mg dimethylamine was added to yield an approximately 10 fold molar excess, and the reaction mixture stirred at room-temperature overnight. The progress of the reaction was measured by thin-layer-chromatography (30% ethyl acetate in hexane).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05739271 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-46c610fd8e2d4ca1946f4ca4cd9a38b4 |
| Source note | uspto-grants-1998_04 |