Methyl iodide → HCID 178480113, compound

HRID 1599392Notes

Reaction equation

HRID 1599392 reaction equation
[NH:1]1[C:13]2[C:4]([S:5][CH:6]=[C:7]3[CH:12]=[CH:11][N:10]=[CH:9][C:8]3=2)=[N:3][S:2]1.[CH3:14][I:15]>CC(C)=O>[I-:15].[CH3:14][N:10]1[CH:11]=[CH:12][C:7]2=[CH:6][S:5][C:4]3[C:13](=[NH+:1][S:2][N:3]=3)[C:8]2=[CH:9]1

Participants

4

Reactant 2

HCID 6328Methyl iodideHCID 18928234HCID 18928234, compound

Product 1

HCID 178480113HCID 178480113, compound

Reagents, catalysts & solvents 1

HCID 180AcetoneSolvent

Procedure

A solution of [1,2,5]thiadiazolo[3',4':2,3]thiopyrano[4,5-c]pyridine (100 mg, 0.5 mmol) and methyliodide (1.5 mmol) in acetone (10 ml) was stirred at room temperature overnight. The precipitate was collected by filtration to give the wanted product in 120 mg (70%) yield.

Workup

  1. filtrationThe precipitate was collected by filtration
  2. customto give the wanted product in 120 mg (70%)
  3. customyield

Sources & evidence

ORD record
ord-491722ab9b4b4535aeecb35ae9a0bd6f
Source dataset
uspto-grants-1998_04
Patent number
US05741788

Reaction notes

Loading…