HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178480113, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 18928234 | HCID 18928234 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 178480113 | HCID 178480113 | — |
Reaction Steps
A solution of [1,2,5]thiadiazolo[3',4':2,3]thiopyrano[4,5-c]pyridine (100 mg, 0.5 mmol) and methyliodide (1.5 mmol) in acetone (10 ml) was stirred at room temperature overnight. The precipitate was collected by filtration to give the wanted product in 120 mg (70%) yield.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05741788 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-491722ab9b4b4535aeecb35ae9a0bd6f |
| Source note | uspto-grants-1998_04 |