HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1599471Generated: November 4, 2026
Oxalyl chloride → 3-(4-Methylphenyl)propanoyl chloride
https://huagongshe.com/reaction/1599471
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | 3-(p-Tolyl)propionic acid | HCID 73927 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 3-(4-Methylphenyl)propanoyl chloride | HCID 13029200 | — |
Reaction Steps
A solution of oxalyl chloride (5 ml) in dichloromethane (5 ml) was added dropwise to a solution of 3-(4-methylphenyl)propionic acid (1.5 g) in dichloromethane (20 ml). The mixture was stirred at 20° C. for 16 hours and then evaporated to give 3-(4-methylphenyl)propionyl chloride as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05741800 |
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| Source dataset | uspto-grants-1998_04 |
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| ORD ID | ord-8003302ee8fe4e75926472882c33d452 |
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| Source note | uspto-grants-1998_04 |
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