1,4-Cyclohexanedimethanamine → 4-Methylbenzylamine

HRID 1599782Notes

Reaction equation

HRID 1599782 reaction equation
[NH2:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH:6]([CH2:9]N)[CH2:5][CH2:4]1>C1(C)C=CC(C)=CC=1>[NH2:1][CH2:2][CH:3]1[CH2:8][CH2:7][CH:6]([CH3:9])[CH2:5][CH2:4]1.[CH3:9][C:6]1[CH:7]=[CH:8][C:3]([CH2:2][NH2:1])=[CH:4][CH:5]=1

Participants

4

Reactant 1

HCID 173541,4-Cyclohexanedimethanamine

Product 2

HCID 660354-MethylbenzylamineHCID 197031994-Methylcyclohexanemethanamine

Reagents, catalysts & solvents 1

HCID 7809P-XyleneSolvent

Procedure

As a result of analysis by gaschromatography, it was found that the yield of 1,4-bis(aminomethyl)cyclohexane was 95.9 mol % and as other products 3.4 mol % of 4-aminomethyl-1-methylcyclohexane, 0.3 mol % of 4-methyl-benzylamine and 0.2 mol % of paraxylene were obtained.

Workup

  1. customAs a result of analysis by gaschromatography, it

Sources & evidence

ORD record
ord-63d912cd8e574637aed728ad30d1abb6
Source dataset
uspto-grants-1998_04
Patent number
US05741928

Reaction notes

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