HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Cyclohexanedimethanamine → 4-Methylbenzylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Cyclohexanedimethanamine | HCID 17354 | — |
| Solvent | P-Xylene | HCID 7809 | — |
| Product | 4-Methylbenzylamine | HCID 66035 | — |
| Product | 4-Methylcyclohexanemethanamine | HCID 19703199 | — |
Reaction Steps
As a result of analysis by gaschromatography, it was found that the yield of 1,4-bis(aminomethyl)cyclohexane was 95.9 mol % and as other products 3.4 mol % of 4-aminomethyl-1-methylcyclohexane, 0.3 mol % of 4-methyl-benzylamine and 0.2 mol % of paraxylene were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05741928 |
| Source dataset | uspto-grants-1998_04 |
| ORD ID | ord-63d912cd8e574637aed728ad30d1abb6 |
| Source note | uspto-grants-1998_04 |