Hydrochloric Acid → HCID 86752443, compound

HRID 1599930Notes

Reaction equation

HRID 1599930 reaction equation
[NH2:1][C:2]1[S:3][CH:4]=[C:5]([CH2:7][CH2:8][C:9]2[CH:19]=[CH:18][C:12]([C:13]([O:15]CC)=[O:14])=[CH:11][CH:10]=2)[N:6]=1.[ClH:20]>>[ClH:20].[NH2:1][C:2]1[S:3][CH:4]=[C:5]([CH2:7][CH2:8][C:9]2[CH:19]=[CH:18][C:12]([C:13]([OH:15])=[O:14])=[CH:11][CH:10]=2)[N:6]=1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 18928616HCID 18928616, compound

Product 1

HCID 86752443HCID 86752443, compound

Procedure

Ester 21-3 (1.5 g, 5.43 mmol) was treated with 6N HCl for 16 h at RT then 16 h at 50°. Concentration provided 21-4 as an off-white solid.

Workup

  1. custom16 h
  2. customat 50°
  3. concentrationConcentration

Sources & evidence

ORD record
ord-5e4c173c18534e6eb6a09e760688e1db
Source dataset
uspto-grants-1998_04
Patent number
US05741796

Reaction notes

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